Zhang S.,Hangzhou Dianzi University |
Jiao Z.,Dongguan University of Technology |
Yao W.,Zhejiang Police College
Journal of Chromatography A | Year: 2014
An active magnetic metal-organic framework (MOF) hybrid material was prepared using a novel in situ solvothermal method in the presence of magnetite (Fe3O4) particles, that holds much promise for large-scale synthesis. MIL-101(Fe), an iron terephthalate with pore structure and high resistance to water and common solvents, was functionalized as a model with superparamagnetic qualities, using Fe3O4. The electrostatic interaction between Fe3O4 and metal ions was thereby used to chemically stabilize magnetic nanoparticles, and thus MOF crystals were uniformly enclosed by Fe3O4 to form a homogeneous magnetic product identified as a Fe3O4/MIL-101 composite. This hybrid material with magnetic susceptibility but with the lowest possible loading amount of Fe3O4 was examined, and its potential application for magnetic solid-phase extraction of six organophosphorus pesticides (OPPs) from human hair and urine samples, followed by gas chromatography analysis, was assessed. The main effect parameters including solution ionic strength, desorption solvent, extraction time and desorption time were investigated in sequence. Under optimized conditions, this method showed low detection limits (0.21-2.28ng/mL), wide linearity, and good precision (1.8-8.7% for intra-day, 2.9-9.4% for inter-day). The matrix interference produced by hair or urine could be effectively eliminated using this method, and satisfactory recoveries of the spiked samples were 76.8-94.5% and 74.9-92.1%, respectively, indicating that the Fe3O4/MIL-101 sorbents are feasible for the analysis of trace analytes from biological samples. © 2014.
Xu Z.,Zhejiang Police College |
Wang C.,Shaoxing University
Journal of Animal and Veterinary Advances | Year: 2012
To investigate the effects of Radix Puerariae water Extract (RPE) on exercise-induced fatigue, 96 mice were randomly divided into four groups: Normal Control (NC), Low dose RPE Treated (LRT), Middle dose RPE Treated (MRT) and High dose RPE Treated (HRT) groups. The mice in the treated groups received RPE (2, 4 and 8 g kg" 1, ig) and the mice in the normal control group received drinking water ig for 4 weeks. The exhaustive swimming time, Blood Lactic Acid (BLA), Blood Urea Nitrogen (BUN), Hemoglobin (Hb) and liver glycogen were determined after swimming test. The results indicated that RPE had significant anti-fatigue effects on mice. It extended the exhaustive swimming time of mice, increased the Hb and liver glycogen contents and decreased BLA and BUN contents. © 2012 Medwell Journals.
Zhonghui Z.,Zhejiang Police College |
Xiaowei Z.,Zhejiang University of Technology |
Fang F.,Zhejiang GongShang University
Saudi Journal of Biological Sciences | Year: 2014
The present study was designed to determine the effects of Ganoderma lucidum polysaccharides (GL-PS) on exhaustive exercise-induced oxidative stress in skeletal muscle tissues of mice. The mice were divided into four groups (three GL-PS administered groups and the control group). The control group was administered with distilled water and GL-PS administered groups were administered with GL-PS (50, 100 and 200. mg/kg body weight per day). After 28. days, the mice performed an exhaustive swimming exercise, along with the determination of superoxide dismutase (SOD), glutathione peroxidase (GPX), catalase (CAT) activities and malondialdehyde (MDA) levels in the skeletal muscle of mice. The results showed that GL-PS could increase antioxidant enzymes activities and decrease the MDA levels in the skeletal muscle of mice. This study provides strong evidence that GL-PS supplementation possessed protective effects against exhaustive exercise-induced oxidative stress. © 2013.
Jin S.,Zhejiang University |
Wang D.-H.,Zhejiang University |
Xu C.,Zhejiang Police College |
Huang Z.-Y.,Zhejiang University
Physics Letters, Section A: General, Atomic and Solid State Physics | Year: 2012
This Letter develops a new staggered car-following model taking into consideration lateral separation effects. Time-to-collision, calculated using visual angle variables, is introduced to describe the lateral separation distance and improve the optimal velocity model. The analytical and numerical results show that the stability of traffic flow can gradually be enhanced with the increase of lateral separation effects. The asymmetry property of traffic flow is also investigated using the new model. The results imply that incorporating lateral separation effects into the car-following model leads to the suppression of traffic jams and greatly enhances the realism of the model. © 2011 Elsevier B.V. All rights reserved.
Ma M.-Y.,Zhejiang Police College
International Journal of Digital Content Technology and its Applications | Year: 2012
The remote examination system has gradually become one of the main areas of educational software design. The paper presents the design and implementation of police and tactics Distance Education Examination System based on .NET techniques. The system implements a simple online examination process, student users can log in, registration, online examinations and inquiries examinations; administrators can manage the papers, test scores.