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Tang L.,Yanaan University | Fu F.,Yanaan University | Gao L.,Yanaan University | Wu Y.,Yanaan University | And 2 more authors.
Zeitschrift fur Anorganische und Allgemeine Chemie | Year: 2011

A new coordination polymer, [Ni(3,4-pybz)2(H2O)] n (1), was hydrothermally synthesized from Ni(NO3) 2·6H2O and an unsymmetrical 3-pyridin-4-yl-benzoic acid (3,4-Hpybz). It was characterized by IR spectroscopy, elemental analysis, thermogravimetric analysis, and single-crystal X-ray diffraction. In complex 1, the 3,4-pybz ligands act as linear linkers to join 4-connected nickel(II) ion nodes, to build a 3D 4-connected twofold interpenetrated 658-cds coordination framework. In addition, the magnetic and thermal properties of complex 1 were also investigated. © 2011 WILEY-VCH Verlag GmbH & Co. KGaA, Weinheim.

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