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Lu Z.-S.,Jiangsu University | Zhu G.-Z.,Jiangsu University | Shi H.-L.,Lianyungang Henrychem Science Co.
Zeitschrift fur Kristallographie - New Crystal Structures | Year: 2013

C9H8Br2O3, orthorhombic, Pbca (no. 61), a = 16.340(2) Å, b = 7.580(1) Å, c = 16.944(2) Å, V = 2098.6 Å3, Z = 8, Rgt(F) = 0.0231, wRref(F 2) = 0.0521, T = 296 K. Source


Zhu G.Z.,Jiangsu University | Lu Z.-S.,Jiangsu University | Shi H.-L.,Lianyungang Henrychem Science Co.
Zeitschrift fur Kristallographie - New Crystal Structures | Year: 2013

C8H8Cl2N2O2, orthorhombic, P212121 (no. 19), a = 3.9327(8) Å, b = 13.537(3) Å, c = 18.301(4) Å, V = 974.3 Å3, Z = 4, Rgt(F) = 0.0214, wRref(F2) = 0.0545, T = 296 K. Source


Xu S.-P.,Jiangsu University | Yang F.-L.,Jiangsu University | Zhu G.-Z.,Jiangsu University | Shi H.-L.,Lianyungang Henrychem Science Co. | Li X.-L.,Jiangsu University
Polyhedron | Year: 2014

A series of complexes, [CuLCl]·1·5H2O (1); [ML2]·X (X = 0, M = Cd, 2a; X = DMF, M = Hg, 2b; X = DMF, M = Ni, 2c); [Cu2(OOCCH3)2L2] ·2CH3OH (3) have been synthesized by microwave solid-state method with a tridentate aroylhydrazone ligand HL (HL = N3- salicyloylpyridine-2-carboxamidrazone). All these compounds were characterized by element analysis, IR, X-ray diffraction and electrochemistry. Crystal analysis revealed that the coordination molecules extended to 3D supramolecular networks through plentiful H-bondings and weak molecular interactions between the ligand moieties and solvent molecules. Meanwhile, these compounds displayed diverse metal or ligand localized electrochemical properties. © 2013 Elsevier Ltd. All rights reserved. Source


Lu Z.-S.,Jiangsu University | Zhu G.-Z.,Jiangsu University | Shi H.-L.,Lianyungang Henrychem Science Co. | Wang X.-S.,Jiangsu University
Zeitschrift fur Kristallographie - New Crystal Structures | Year: 2014

C14H19NO4, monoclinic, C2/c (no. 15), a = 30.10(1) Å, b = 5.308(2) Å, c = 20.369(8) Å, β = 117.027(6)°, V = 2898.5 Å3, Z = 8, Rgt(F) = 0.0449, wRref(F2) = 0.1336, T = 296 K. © 2014 by Walter de Gruyter Berlin/Boston. Source


Zhu G.-Z.,Jiangsu University | Lu Z.-S.,Jiangsu University | Shi H.-L.,Lianyungang Henrychem Science Co. | Wang X.-S.,Jiangsu University
Zeitschrift fur Kristallographie - New Crystal Structures | Year: 2013

C9H7F3N2S, monoclinic, P2 1/c (no. 14), a = 8.695(4) Å, b = 4.676(2) Å, c = 24.13(1) Å, β = 97.861(4)°, V = 972.0 Å3, Z = 4, Rgt(F) = 0.0386, wRref(F2) = 0.1074, T = 296 K. © by Oldenbourg Wissenschaftsverlag, München. Source

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