Integrated Test Range ITR

Chandipur, India

Integrated Test Range ITR

Chandipur, India
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Das S.,Indian School of Mines | Sahu S.K.,Integrated Test Range ITR | Oraon R.,Indian School of Mines | Routray P.C.,Integrated Test Range ITR | And 2 more authors.
Bulletin of Materials Science | Year: 2017

Microwave-Absorbing materials based on reduced graphene oxide (r-GO)/strontium titanate were prepared by embedding in epoxy matrix. R-GO and strontium titanate were synthesized and characterized before composite fabrication. Microstructures of the constituent elements were studied by scanning electron microscopy and X-ray diffraction (XRD). Microwave absorption capabilities of the composite absorbers were investigated using a Vector Network Analyser in the range 8-12 GHz. A maximum reflection loss of -7.5 and -16.4 dB was obtained at 9.3 and 12.08 GHz, respectively, for 2% (w/w) r-GO-loaded epoxy composites. A maximum attenuation of -12.8 dB at 9.3 GHz was obtained for the strontium titanate/epoxy composite. However, double-layer composite with r-GO/strontium titanate/epoxy composition showed the maximum reflection loss of -15.1 dB at 9.47 GHz and -9.65 dB at 12.3 GHz. All the results are discussed in terms of complex permeability and permittivity. The study revealed that intrinsic conductivity and polarization of the r-GO particles and dielectric polarization of the strontium titanate within epoxy matrix contribute to the microwave absorption.


Das S.,Indian School of Mines | Nayak G.C.,Indian School of Mines | Sahu S.K.,Integrated Test Range ITR | Routray P.C.,Integrated Test Range ITR | And 2 more authors.
Journal of Magnetism and Magnetic Materials | Year: 2014

Zinc substituted ferrite powders Me0.5Zn0.5Fe2O4 (Me=Co, Mn and Ni) were prepared by the sol-gel auto-combustion method. The present study highlights development of Single layer and double layer composite microwave absorbing materials using Ferrites, Titanium dioxide and Epoxy matrix. Moreover microwave absorption property, i.e. reflection loss evaluated at X-band frequency. XRD analysis of the filler particles were carried out to evaluate crystal structure, average crystallite diameter. Morphology of the filler particles were studied with FESEM. Hysteresis behavior of the ferrites samples were studied with Vibrating Sample Magnetometer. The most important parameter governing the absorption properties of microwave absorbers i.e. permittivity and permeability studied in a vector network analyzer. Measured reflection loss value of single-layer NiZn-ferrite based microwave absorber reaches -11.2 dB at 12.05 GHz. Whereas, reflection loss value of double-layer CoZn-ferrite/ TiO2 based microwave absorber reaches -24.3 dB at 12.02 GHz. The result shows that microwave absorption property and bandwidth of absorption of double-layer microwave absorber was found to improve comparison to single layer. © 2014 Elsevier B.V.


Das S.,Integrated Test Range ITR | Das S.,Indian School of Mines | Chandra Nayak G.,Indian School of Mines | Sahu S.K.,Integrated Test Range ITR | Oraon R.,Indian School of Mines
Journal of Magnetism and Magnetic Materials | Year: 2015

This work explored the microwave absorption capability of Graphene Oxide and Graphene Oxide coated with FeCoB for stealth technology. Epoxy based microwave absorbing materials were prepared with 30% loading of Graphene Oxide, FeCoB alloy and Graphene Oxide coated with FeCoB. Graphene Oxide and FeCoB were synthesized by Hummer's and Co-precipitation methods, respectively. The filler particles were characterized by FESEM, XRD and Vibrating Sample Magnetometer techniques. Permittivity, permeability and reflection loss values of the composite absorbers were measured with vector network analyzer which showed a reflection loss value of -7.86 dB, at 10.72 GHz, for single layered Graphene Oxide/Epoxy based microwave absorbers which can be correlated to the absorption of about 83.97% of the incident microwave energy. Reflection loss value of FeCoB/Epoxy based microwave absorber showed -13.30 dB at 11.67 GHz, which corresponded to maximum absorption of 93.8%. However, reflection loss values of Graphene Oxide coated with FeCoB/Epoxy based single-layer absorber increased to -22.24 dB at 12.4 GHz which corresponds to an absorption of 99% of the incident microwave energy. © 2015 Elsevier B.V. All rights reserved.

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