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Ujjain S.K.,Indian Institute of Technology Kanpur | Bhatia R.,Institute Of Home Economics | Ahuja P.,University of Delhi | Attri P.,Kwangwoon University
PLoS ONE | Year: 2015

We report the functionalization of multiwalled carbon nanotubes (MWCNT) via the 1,3-dipolar [3+2] cycloaddition of aromatic azides, which resulted in a detangled CNT as shown by transmission electron microscopy (TEM). Carboxylic moieties (-COOH) on aromatic azide result in highly stable aqueous dispersion (max. conc. ∼ 10 mg/mL H2O), making the suitable for inkjet printing. Printed patterns on polyethylene terephthalate (PET) flexible substrate exhibit low sheet resistivity ∼65 Ω. cm, which is attributed to enhanced conductivity. Fabricated Supercapacitors (SC) assembled using these printed substrates exhibit good electrochemical performance in organic as well as aqueous electrolytes. High energy and power density (57.8 Wh/kg and 0.85 kW/kg) in 1M H2SO4 aqueous electrolyte demonstrate the excellent performance of the proposed supercapacitor. Capacitive retention varies from ∼85-94% with columbic efficiency ∼95% after 1000 charge/discharge cycles in different electrolytes, demonstrating the excellent potential of the device for futuristic power applications. Copyright © 2015 Ujjain et al. This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited. Source


Manzar M.D.,Jamia Millia Islamia University | Zannat W.,Indian Institute of Technology Guwahati | Kaur M.,Institute Of Home Economics | Hussain M.E.,Jamia Millia Islamia University
International Journal of Adolescent Medicine and Health | Year: 2015

Purpose: Assessment of the influence of gender and increasing years at university on sleep health of students. Methods: Four hundred and eighteen students from different streams across years of undergraduate to postgraduate courses participated. Descriptive statistics, test of differences, and correlation were used. The sleep health data comprised of subjective evaluation using a questionnaire and personal interviews. Results: Overall, 43.1% had sleep problems, females were more affected (51.67% vs. 48.33% in males) but were early bed goers. The prevalence of circadian rhythm sleep disorder (11.6% vs. 9.5%) and delayed sleep phase syndrome (4.5% vs. 2.7%) was slightly higher in males. The daytime dysfunction and hypnotic use significantly differed in students of the same class among gender. Bedtime got significantly delayed along years [H(2)=29.769, p<0.001], and hypnotic use [H(2)=8.807, p=0.012] differed significantly among them. The moderate-very strong correlational statistics among sleep health elements was very similar across gender and years of university education. However, more pronounced influence of years of university education than gender was seen in the significant differences for correlated correlation among sleep health parameters. Conclusion: Gender and years of university education influence sleep among university students both separately and concomitantly. © 2015 by De Gruyter. Source


Tripathi B.,Indian Agricultural Research Institute | Bhatia R.,Institute Of Home Economics | Bhatia R.,University of Delhi | Pandey A.,University of Delhi | And 5 more authors.
Journal of Chemistry | Year: 2014

Antioxidant and nematicidal properties were evaluated for R. emodi extractives which are extracted by standardizing and adopting accelerated solvent extraction (ASE) method along with traditional Soxhlet extraction. The extracted material was separated using flash chromatography and the separation conditions and solvents were standardized for the extracted plant constituents. The purity was detected by using analytical reverse phase high pressure liquid chromatography (HPLC). LC-MS/MS detection in the direct infusion mode of the isolated, purified products afforded four anthraquinones, characterized by their infrared spectra (IR) and 1H spectra as chrysophanol, physcion, emodin, and aloe-emodin. Five antraquinone glucoside derivatives and piceatannol-3-O-β-d-glucopyranoside have also been detected from the extracted product. During in vitro evaluation the antioxidant potential of methanolic crude extract (CE1) was the highest, followed by ethyl acetate crude extract (CE2) and chloroform extract (CE3) in DPPH radical scavenging activity. The CE1 also demonstrated outstanding nematicidal activity as compared with other extracts, pure anthraquinones, and even positive control azadirachtin. The study conclusively demonstrated the antioxidant potential of R. emodi extracts and also its ability in extenuating the Meloidogyne incognita (root-knot nematode). The bioassay results can be extrapolated to actual field condition and clinical studies. © 2014 Brijesh Tripathi et al. Source


Sharma R.,Medicity | Gulati S.,Diabetes Foundation India | Joshi S.R.,Lilavati and Bhatia Hospital | Sharma V.,Ministry of Science and Technology | And 28 more authors.
Diabetes Technology and Therapeutics | Year: 2011

India is undergoing rapid nutritional transition, resulting in excess consumption of calories, saturated fats, trans fatty acids, simple sugars, salt and low intake of fiber. Such dietary transition and a sedentary lifestyle have led to an increase in obesity and diet-related non-communicable diseases (type 2 diabetes mellitus [T2DM], cardiovascular disease [CVD], etc.) predominantly in urban, but also in rural areas. In comparison with the previous guidelines, these consensus dietary guidelines include reduction in the intake of carbohydrates, preferential intake of complex carbohydrates and low glycemic index foods, higher intake of fiber, lower intake of saturated fats, optimal ratio of essential fatty acids, reduction in trans fatty acids, slightly higher protein intake, lower intake of salt, and restricted intake of sugar. While these guidelines are applicable to Asian Indians in any geographical setting, they are particularly applicable to those residing in urban and in semi-urban areas. Proper application of these guidelines will help curb the rising "epidemics" of obesity, the metabolic syndrome, hypertension, T2DM, and CVD in Asian Indians. © 2011 Mary Ann Liebert, Inc. Source


Ujjain S.K.,Indian Institute of Technology Kanpur | Ujjain S.K.,University of Delhi | Ahuja P.,University of Delhi | Bhatia R.,Institute Of Home Economics | And 3 more authors.
Journal of Nanoscience and Nanotechnology | Year: 2015

Various synthetic methods were employed on a single precursor to synthesize magnetic cobalt dithiocarbamate (Co(dtc-SB)) coordination polymer nanoparticles (MCP NPs) having different morphologies. When subjected to hydrothermal method, the precursor led to the formation of nanosheets (NSs) of MCP (100×80 nm), whereas the same precursor when set to slow diffusion precipitation, formed nanowires (NWs) with 30 nm diameter. Further, on micro-emulsion ultrasonication, uniform MCP nanocubes (NCs) ∼5 nm were obtained. MCP NPs are weakly ferromagnetic in nature with a narrow hysteresis loop opening. In addition, the magnetic properties of MCP NPs are shown to be highly dependent on size. Further, the antimicrobial activity of MCP NPs against various microbes was also shown to be highly size dependent. The biocompatible MCP NCs were found to have the lowest minimum inhibitory concentration (MIC) value of 6.25 μg/ml against S. aureus and K. pneumoneae, which demonstrate that NPs are equally effective against both gram positive and gram negative bacteria. Copyright © 2015 American Scientific Publishers. Source

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