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Cao L.,Center for Chemical Methodologies and Library Development | MacIejewski J.P.,Center for Chemical Methodologies and Library Development | Elzner S.,Center for Chemical Methodologies and Library Development | Amantini D.,Center for Chemical Methodologies and Library Development | Wipf P.,Center for Chemical Methodologies and Library Development
Organic and Biomolecular Chemistry | Year: 2012

The intramolecular Staudinger-aza-Wittig reaction is used for a general synthesis of 1,2,5,6-tetrahydro-1,2,4-triazines, a structural motif reported for the natural product noelaquinone. The DEF moiety of noelaquinone was obtained in 13 steps and 2% overall yield, and the structure of the synthetic product was confirmed by X-ray analysis. © 2012 The Royal Society of Chemistry. Source

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